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从抗生素生产废水中回收丁醇-醋酸丁酯的工艺方法
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2020-11-14
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本发明涉及一种从抗生素生产废水中回收丁醇-醋酸丁酯的工艺方法。丁醇-醋酸丁酯含量为1-5%(质量分数)的废水经过精馏塔塔釜液预热,再经换热器加热后达到80-85℃进入闪蒸塔,闪蒸塔塔顶馏出液进入精馏塔进行分离。精馏塔塔顶的列管式换热器连接减压器,使得精馏塔和列管式换热器壳程维持在绝对压力35kPa以下。塔顶蒸汽被冷凝后进入分相罐,轻相进入待检罐,重相回流,塔釜液经冷却到30-35℃后排放。本发明提高了丁醇和醋酸丁酯的回收率,通过减压蒸馏和热量综合利用,能够降低能耗,具有显著的实用性和经济性。
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从抗生素生产废水中回收丁醇-醋酸丁酯的工艺方法
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